北京世紀(ji)森朗聚(ju)合反(fan)(fan)應(ying)小試反(fan)(fan)應(ying)器(qi)(qi)系(xi)統，該反(fan)(fan)應(ying)器(qi)(qi)系(xi)統主要用于聚(ju)合反(fan)(fan)應(ying)的(de)條件探究及工藝優化。裝置包括液體(ti)進料(liao)/配料(liao)系(xi)統、攪拌反(fan)(fan)應(ying)系(xi)統、產物收(shou)集系(xi)統、尾氣(qi)處理系(xi)統及控制系(xi)統等

合(he)成反應(ying)小(xiao)試反應(ying)器(qi)(qi)(qi)系(xi)統，反應(ying)釜(fu)使(shi)用(yong)壓力12.6 MPa，設(she)計壓力20 MPa，使(shi)用(yong)溫(wen)(wen)(wen)度(du)(du)(du)380 ℃，設(she)計溫(wen)(wen)(wen)度(du)(du)(du)400 ℃，溫(wen)(wen)(wen)度(du)(du)(du)控制(zhi)精(jing)度(du)(du)(du)小(xiao)于(yu)±;1℃，壓力顯示精(jing)度(du)(du)(du)小(xiao)于(yu)±0.5%，液體(ti)流量控制(zhi)精(jing)度(du)(du)(du)小(xiao)于(yu)±1%。反應(ying)釜(fu)采用(yong)電(dian)加熱(re)(re)，內盤管導熱(re)(re)油(you)撤熱(re)(re)。配料(liao)物料(liao)經進(jin)(jin)料(liao)泵輸送到攪拌反應(ying)器(qi)(qi)(qi)，從(cong)反應(ying)器(qi)(qi)(qi)釜(fu)底出來的產(chan)物進(jin)(jin)入產(chan)品罐，氣相進(jin)(jin)入冷凝系(xi)統。裝(zhuang)置反應(ying)釜(fu)釜(fu)蓋、釜(fu)體(ti)材質、內部構件、攪拌驅動(dong)器(qi)(qi)(qi)等高溫(wen)(wen)(wen)區域，要求材質均為TA2，其余金屬器(qi)(qi)(qi)件部分316L材質。